ICI D2138 synthesis
- Product Name:ICI D2138
- CAS Number:140841-32-3
- Molecular formula:C23H24FNO4
- Molecular Weight:397.44
29943-42-8
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 1.) n-BuLi / 1.) THF, hexane, -70 deg C, 1 h, 2.) THF, hexane, from -70 to 0 deg C, 3 h
2: 1.) NaH / 1.) DMF, 5 deg C, 1 h, 2.) DMF, from 5 deg C to RT, overnight
3: 95 percent / H2 / 10percent Pd/C / ethanol / 2 h
4: 88 percent / K2CO3 / dimethylformamide / Ambient temperature
References:
Crawley;Dowell;Edwards;Foster;McMillan;Walker;Waterson [Journal of Medicinal Chemistry,1992,vol. 35,# 14,p. 2600 - 2609]
461-96-1
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130722-44-0
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![2H-Pyran-4-ol, 4-[3-fluoro-5-(phenylmethoxy)phenyl]tetrahydro-](/CAS/20210305/GIF/130723-10-3.gif)
130723-10-3
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140841-32-3
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