ETHYL-O-TOLYL KETONE synthesis
- Product Name:ETHYL-O-TOLYL KETONE
- CAS Number:2040-14-4
- Molecular formula:C10H12O
- Molecular Weight:148.2
61017-92-3
2040-14-4
1-(p-formyl)ethanol (1 mmol) was used as starting material with chloramine-T (1 mmol) and In(OTf)3 (0.3 mmol) in a 100 mL round-bottomed flask fitted with a magnetic stirrer and dissolved in acetonitrile (10 mL). The reaction mixture was heated and refluxed under argon protection for 3 h. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the mixture was cooled to room temperature and the solvent was removed by rotary evaporator. The residue was purified by fast column chromatography on silica gel. The final product was analyzed by spectroscopy for structural confirmation.
95-46-5
307 suppliers
$10.00/10 g
2040-14-4
74 suppliers
$36.00/250mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: n-butyllithium
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux
References:
Hu, Bin;Meng, Meng;Jiang, Shanshan;Deng, Weiping [Chinese Journal of Chemistry,2012,vol. 30,# 6,p. 1289 - 1294]
61017-92-3
6 suppliers
$809.00/1g
2040-14-4
74 suppliers
$36.00/250mg
118-90-1
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$13.00/1g
2386-64-3
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$45.00/5ml
2040-14-4
74 suppliers
$36.00/250mg
529-19-1
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$17.89/50g
75-03-6
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2040-14-4
74 suppliers
$36.00/250mg
15898-37-0
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107-12-0
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$47.00/250ml
2040-14-4
74 suppliers
$36.00/250mg