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ChemicalBook CAS DataBase List Benzyl ether
103-50-4

Benzyl ether synthesis

14synthesis methods
As a by-product in the preparation of benzyl alcohol by hydrolysis of benzyl chloride; by using a concentrated caustic instead of carbonate, yields can be improved to 50% or higher.
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Yield:103-50-4 98%

Reaction Conditions:

with triethylsilane;silver tetrafluoroborate at 20; for 0.0833333 h;Catalytic behavior;Green chemistry;Reagent/catalyst;Temperature;

Steps:

4 Example 4
Example 4:1% AgBF4 (0.05 mmol, 9.7 mg) was added to the 100 mL reaction flask in turn.Further add benzaldehyde (50 mmol, 5.360 g) and triphenylsilane (50 mmol, 13.6591 g),The reaction was stirred at room temperature for 5 minutes, and after completion of the reaction, direct distillation under reduced pressure (2 mmHg, 90 ° C) gave the desired product.The yield was 98%. The product structure characterization data is the same as in Example 1.

References:

Xuzhou Medical University;Xu Zhou;Liang Ting;Mi Jiajia;Zhai Rongliang;Shi Yanfen CN108164486, 2018, A Location in patent:Paragraph 0043; 0044; 0045; 0046

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