5-AZABENZIMIDAZOLE synthesis
- Product Name:5-AZABENZIMIDAZOLE
- CAS Number:272-97-9
- Molecular formula:C6H5N3
- Molecular Weight:119.12
54-96-6
362 suppliers
$5.00/100mg
1758-73-2
462 suppliers
$18.00/25g
272-97-9
133 suppliers
$9.00/250mg
Yield: 90%
Reaction Conditions:
in water at 60; for 1 h;
Steps:
General procedure.
General procedure: A typical reaction mixturecontaining 1a-1i (4 mmol), 2 (7.2 mmol), and 2 mLH2O was stirred at 60°C for a certain time until reactioncompletion (by TLC). After cooling, a precipitateformed and was fi ltered off and washed with water.The crude product was purifi ed by recrystallizationfrom water. All products are known compounds. Theywere characterized by melting points, 1H and 13CNMR spectra, and HRMS, which were consistent withpublished data [23, 24].
References:
Huang, W.-H.;Jin, Y.-J.;Ma, L.-F.;Wu, Y.;Zhou, L.-H. [Russian Journal of Organic Chemistry,2021,vol. 57,# 5,p. 825 - 830][Zh. Org. Khim.]
54-96-6
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$5.00/100mg
124-38-9
130 suppliers
$175.00/23402
272-97-9
133 suppliers
$9.00/250mg
54-96-6
362 suppliers
$5.00/100mg
64-18-6
1112 suppliers
$22.12/250ML
272-97-9
133 suppliers
$9.00/250mg
54-96-6
362 suppliers
$5.00/100mg
122-51-0
506 suppliers
$10.00/5ml
272-97-9
133 suppliers
$9.00/250mg
