2-Iodotoluene synthesis
- Product Name:2-Iodotoluene
- CAS Number:615-37-2
- Molecular formula:C7H7I
- Molecular Weight:218.04
16419-60-6
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615-37-2
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$5.00/5g
Yield:615-37-2 88%
Reaction Conditions:
with potassium fluoride;iodine in 1,4-dioxane at 80; for 1 h;
Steps:
General procedure
General procedure: A mixture of the arylboronic acid (0.55mmol), KF (96mg, 1.65mmol) and I2 (127mg, 0.50mmol) in 1,4-dioxane (5mL) was stirred at 80°C for 1h. Then it was filtered through silica gel, eluting with Et2O (10mL) and the solvent was removed by rotary evaporation. When necessary, the product was purified by chromatography on silica gel (petroleum ether/Et2O 98:2).
References:
Tramutola, Francesco;Chiummiento, Lucia;Funicello, Maria;Lupattelli, Paolo [Tetrahedron Letters,2015,vol. 56,# 9,p. 1122 - 1123]
2093-46-1
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615-37-2
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108-88-3
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615-37-2
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118-90-1
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615-37-2
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95-46-5
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615-37-2
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