4-氟苯肼鹽酸鹽(823-85-8)核磁圖(¹³CNMR)

產(chǎn)品名稱:4-氟苯肼鹽酸鹽

CAS:823-85-8

分子式:C6H8ClFN2

分子量: 162.59

InChI:InChI=1S/C6H7FN2.ClH/c7-5-1-3-6(9-8)4-2-5;/h1-4,9H,8H2;1H

InChIKey: FEKUXLUOKFSMRO-UHFFFAOYSA-N

Smiles:N(C1=CC=C(F)C=C1)N.[H]Cl

Mass

MS-NW-6734          
p-fluorophenylhydrazine hydrochloride
C6H7FN2 HCl         (Mass of molecular ion:    126)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      16.0       2.4
      17.0       2.7
      17.5       1.0
      18.0       3.4
      26.0       2.1
      27.0       2.4
      28.0       5.9
      29.0      13.9
      30.0       3.3
      31.0       8.9
      33.0       2.4
      35.0      12.8
      36.0      47.7
      37.0       6.5
      38.0      15.1
      39.0       8.3
      40.0       2.1
      41.0       1.3
      45.0       1.7
      49.0       2.7
      50.0      15.8
      51.0      14.3
      52.0       7.3
      53.0       1.4
      55.0       1.2
      56.0       6.5
      57.0      28.4
      58.0       2.3
      60.0       1.2
      61.0       6.3
      62.0       8.6
      63.0      14.8
      64.0       4.8
      65.0       1.9
      68.0       5.1
      69.0       7.4
      70.0       7.9
      71.0       2.3
      73.0       2.3
      74.0       8.2
      75.0      24.1
      76.0       4.5
      77.0      16.3
      78.0       2.9
      80.0       1.1
      81.0       8.9
      82.0      14.1
      83.0      96.9
      84.0      11.1
      89.0       4.2
      90.0       3.7
      91.0       1.3
      92.0       1.0
      93.0       1.5
      94.0       3.0
      95.0      24.9
      96.0      21.3
      97.0       7.3
      98.0       4.5
      99.0       1.1
     108.0       2.9
     109.0      15.1
     110.0      73.9
     111.0      15.9
     112.0       1.1
     123.0       1.3
     124.0       3.8
     125.0       3.6
     126.0     100.0
     127.0       7.6

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₇ F N₂	0.034 g : 0.5 ml DMSO-d₆
p-fluorophenylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.39
      B             8.3
      C             7.136
      D             7.090

     Hz     ppm     Int.

   4151.83  10.389    558
   2866.37   7.173     36
   2863.08   7.164    382
   2860.69   7.158    142
   2856.48   7.148    209
   2854.10   7.142   1000
   2852.27   7.137    200
   2850.80   7.134    144
   2849.52   7.131     72
   2847.87   7.126    198
   2845.31   7.120    866
   2842.19   7.112    171
   2838.53   7.103    810
   2836.15   7.097    257
   2833.77   7.091    882
   2831.39   7.085    269
   2829.37   7.080    380
   2826.99   7.074    156
   2824.61   7.068    300
   2821.50   7.060     40

in DMSO-d6