1,2,4,5-四異丙基硫苯(74542-69-1)核磁圖(¹HNMR)

產(chǎn)品名稱:1,2,4,5-四異丙基硫苯

CAS:74542-69-1

分子式:C18H30S4

分子量: 374.69

InChI:InChI=1S/C18H30S4/c1-11(2)19-15-9-17(21-13(5)6)18(22-14(7)8)10-16(15)20-12(3)4/h9-14H,1-8H3

InChIKey: GTFNUNQIHYSXTJ-UHFFFAOYSA-N

Smiles:C1(SC(C)C)=CC(SC(C)C)=C(SC(C)C)C=C1SC(C)C

¹HNMR

¹³CNMR

Mass

MS-IW-4612          
1,2,4,5-tetrakis(isopropylthio)benzene
C18H30S4            (Mass of molecular ion:    374)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      27.0       3.1
      39.0       1.8
      41.0       7.7
      42.0       1.4
      43.0      15.1
      96.0       1.0
     101.0       1.2
     109.0       1.4
     127.0       1.3
     139.0       1.6
     140.0       2.7
     141.0       3.3
     142.0       1.1
     171.0       3.5
     172.0       7.2
     173.0       4.0
     174.0       2.7
     179.0       1.3
     180.0       2.4
     199.0       1.3
     203.0       1.1
     204.0       3.4
     205.0       6.0
     206.0      12.1
     207.0       2.2
     208.0       2.2
     213.0       1.3
     214.0       1.9
     215.0       1.6
     216.0       1.3
     217.0       1.2
     222.0       2.1
     231.0       1.3
     241.0       1.7
     247.0       3.8
     248.0      11.7
     249.0       2.2
     250.0       2.1
     256.0       2.8
     257.0       1.0
     258.0       1.2
     289.0       3.6
     290.0      12.1
     291.0       2.5
     292.0       2.3
     298.0       1.0
     331.0       5.5
     332.0      15.8
     333.0       4.0
     334.0       3.2
     374.0     100.0
     375.0      23.1
     376.0      20.2
     377.0       4.2
     378.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₈ H₃₀ S₄	0.037 g : 0.5 ml CDCl₃
1,2,4,5-tetrakis(isopropylthio)benzene

    Assign.     Shift(ppm)

      A             7.299
      B             3.452
      C             1.332

     Hz     ppm     Int.

   2917.24   7.300    215
   1393.31   3.487     32
   1386.72   3.470     81
   1380.00   3.454    111
   1373.41   3.437     84
   1366.70   3.420     35
    536.01   1.342    997
    529.30   1.325   1000

in CDCl3