N-芐基酞酰亞胺(2142-01-0)核磁圖(¹³CNMR)

產(chǎn)品名稱:N-芐基酞酰亞胺

CAS:2142-01-0

分子式:C15H11NO2

分子量: 237.25

InChI:InChI=1S/C15H11NO2/c17-14-12-8-4-5-9-13(12)15(18)16(14)10-11-6-2-1-3-7-11/h1-9H,10H2

InChIKey: WITXFYCLPDFRNM-UHFFFAOYSA-N

Smiles:C1(=O)C2=C(C=CC=C2)C(=O)N1CC1=CC=CC=C1

Mass

MS-NW-6309          
N-benzylphthalimide
C15H11NO2           (Mass of molecular ion:    237)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       2.9
      27.0       1.8
      28.0       1.3
      38.0       1.8
      39.0       6.7
      41.0       1.2
      50.0      14.6
      51.0      13.0
      52.0       2.7
      62.0       1.2
      63.0       4.1
      64.0       1.7
      65.0       9.0
      74.0       4.2
      75.0       6.6
      76.0      24.2
      77.0      30.9
      78.0      14.2
      79.0       1.6
      89.0       5.0
      90.0       4.5
      91.0      11.6
      92.0       1.0
     102.0       4.2
     103.0       4.0
     104.0      55.9
     105.0      19.2
     106.0       3.4
     130.0      11.6
     131.0       2.7
     132.0       3.9
     133.0       5.7
     152.0       3.0
     153.0       1.7
     160.0       3.7
     164.0       2.5
     165.0       4.1
     166.0       1.6
     180.0      11.6
     181.0       4.1
     190.0       1.2
     192.0       1.1
     193.0       1.2
     208.0      19.7
     209.0      21.6
     210.0       3.3
     219.0      29.1
     220.0       6.3
     236.0       4.7
     237.0     100.0
     238.0      16.9
     239.0       1.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₅ H₁₁ N O₂	0.047 g : 0.5 ml CDCl₃
N-benzylphthalimide

    Assign.     Shift(ppm)

      A             7.82
      B             7.66
      C          7.53 to 7.17
      D             4.834

     Hz     ppm     Int.

    705.44   7.877    235
    702.56   7.845    144
    701.81   7.837    159
    700.63   7.824    155
    699.19   7.807    286
    696.88   7.782    423
    696.50   7.777    451
    694.88   7.759     66
    693.94   7.749    145
    693.50   7.744    193
    692.75   7.736    152
    690.19   7.707    429
    689.81   7.703    439
    687.50   7.677    217
    686.06   7.661    160
    684.88   7.648    162
    684.13   7.639    141
    681.25   7.607    237
    671.44   7.498     54
    669.50   7.476     56
    667.25   7.451    121
    666.69   7.445    108
    666.13   7.438     93
    664.88   7.424     99
    664.00   7.415    122
    662.94   7.403    227
    660.94   7.380    284
    659.00   7.359    154
    658.56   7.354    159
    657.19   7.338    208
    655.50   7.320    319
    654.75   7.311    329
    653.44   7.297    230
    652.31   7.284    165
    651.06   7.270    225
    650.00   7.258    291
    647.75   7.233    339
    646.06   7.214     51
    644.88   7.201     30
    644.38   7.195     35
    433.00   4.835   1000

in CDCl3