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144-48-9

2-碘乙酰胺(144-48-9)核磁圖(1HNMR)

產品名稱:2-碘乙酰胺

CAS:144-48-9

分子式:C2H4INO

分子量: 184.96

InChI:InChI=1S/C2H4INO/c3-1-2(4)5/h1H2,(H2,4,5)

InChIKey: PGLTVOMIXTUURA-UHFFFAOYSA-N

Smiles:C(N)(=O)CI

  • 圖譜
    Mass 

    MS-NW-5004          
iodoacetamide
C2H4INO             (Mass of molecular ion:    185)


       Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          12.0       2.8
      13.0       4.8
      14.0      18.6
      15.0      13.1
      16.0       6.1
      17.0       2.7
      18.0       5.0
      26.0       1.6
      27.0       4.5
      28.0      25.9
      29.0       5.1
      30.0      49.2
      31.0       1.2
      38.0       2.5
      39.0       3.0
      40.0      11.6
      41.0       8.6
      42.0      59.4
      43.0       4.8
      44.0      48.8
      58.0     100.0
      59.0       3.5
     127.0      27.3
     128.0       5.0
     139.0       1.4
     140.0       2.2
     141.0      11.5
     142.0      14.8
     143.0       1.3
     167.0       3.0
     168.0       1.6
     169.0       1.8
     185.0      22.7

400 MHz in DMSO-d6

parameter in D20

  • 圖譜

    1H NMR 399.65 MHz
    C2 H4 I N O 0.035 g : 0.5 ml DMSO-d6
    iodoacetamide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A     *1      7.64
      B     *1      7.08
      C             3.578
  

         Hz     ppm     Int.


       3055.54   7.646     60
   2828.86   7.079     69
   1430.66   3.580   1000
   1429.81   3.578    944

  • 圖譜

    1H NMR 300 MHz
    C2 H4 I N O 0.046 g : 0.5 ml D2O
    iodoacetamide
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         3.779
  

         Hz     ppm     Int.


       1133.70   3.779   1000

in DMSO-d6

  • 圖譜

KBr disc

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nujol mull

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GAMMA-RAY IRRAD. AT 77K

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