1,8-Diamino-3,6-dioxaoctane(929-59-9) ¹³C NMR

Product Name1,8-Diamino-3,6-dioxaoctane

CAS 929-59-9

Molecular FormulaC6H16N2O2

Molecular Weight148.2

InChIInChI=1S/C6H16N2O2/c7-1-3-9-5-6-10-4-2-8/h1-8H2

InChIKey IWBOPFCKHIJFMS-UHFFFAOYSA-N

SmilesC(OCCN)COCCN

Request For Quotation

1,8-Diamino-3,6-dioxaoctane(929-59-9) <sup>13</sup>C NMR
Mass

MS-IW-9153          
2,2'-(ethylenedioxy)diethylamine
C6H16N2O2           (Mass of molecular ion:    148)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.9
      17.0       1.3
      18.0      18.1
      27.0       4.6
      28.0      12.2
      29.0       4.5
      30.0     100.0
      31.0      14.9
      41.0       2.9
      42.0      11.0
      43.0      22.1
      44.0      59.3
      45.0       9.2
      55.0       1.3
      56.0       4.8
      57.0       3.5
      58.0       4.5
      59.0       2.4
      60.0       3.6
      61.0      29.1
      62.0       3.5
      68.0       2.7
      69.0       6.6
      70.0       1.5
      72.0      12.0
      73.0       1.1
      74.0       1.3
      81.0       1.1
      84.0       1.7
      86.0       1.2
      87.0       7.1
      88.0       1.6
      89.0      26.7
      90.0       1.3
     102.0       3.8
     106.0       6.4
     119.0      24.6
     120.0       1.5

400 MHz in CDCl3

1,8-Diamino-3,6-dioxaoctane(929-59-9) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₆ H₁₆ N₂ O₂	0.05 ml : 0.5 ml CDCl₃
2,2'-(ethylenedioxy)diethylamine

    Assign.     Shift(ppm)

      A             3.635
      B             3.514
      C             2.866
      D             1.28

     Hz     ppm     Int.

   1452.88   3.636   1000
   1409.79   3.528    363
   1404.54   3.515    486
   1399.29   3.502    365
   1150.63   2.880    130
   1145.63   2.867    182
   1140.63   2.855    116
    509.77   1.276     96

in CDCl3