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METHYL 4-BENZYLOXY-3-METHOXYBENZOATE

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Products Intro: Product Name:METHYL 4-BENZYLOXY-3-METHOXYBENZOATE
CAS:56441-97-5
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CAS:56441-97-5
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CAS:56441-97-5

METHYL 4-BENZYLOXY-3-METHOXYBENZOATE manufacturers

METHYL 4-BENZYLOXY-3-METHOXYBENZOATE Basic information
Product Name:METHYL 4-BENZYLOXY-3-METHOXYBENZOATE
Synonyms:METHYL BENZYL VANILLATE;METHYL 4-BENZYLOXY-3-METHOXYBENZOATE;RARECHEM AL BF 0064;4-Benzyloxy-3-Methoxybenzoic Acid Methyl Ester;Benzoic acid, 3-Methoxy-4-(phenylMethoxy)-, Methyl ester;-3-methoxybenzoate;Methyl 4-(benzyloxy);3-?methoxy-?4-?(phenylmethoxy)?-?, methyl ester Benzoic acid
CAS:56441-97-5
MF:C16H16O4
MW:272.3
EINECS:
Product Categories:Aromatic Esters
Mol File:56441-97-5.mol
METHYL 4-BENZYLOXY-3-METHOXYBENZOATE Structure
METHYL 4-BENZYLOXY-3-METHOXYBENZOATE Chemical Properties
Boiling point 400.1±30.0 °C(Predicted)
density 1.153±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
solubility DCM, Ethyl Acetate
form Solid
color Off-White
Safety Information
MSDS Information
METHYL 4-BENZYLOXY-3-METHOXYBENZOATE Usage And Synthesis
Uses4-Benzyloxy-3-methoxybenzoic Acid Methyl Ester is an intermediate in the synthesis of Clomiphene (C587025), an synthetic estrogen agonist-antagonist.
Synthesis
Methyl vanillate

3943-74-6

Benzyl bromide

100-39-0

METHYL 4-BENZYLOXY-3-METHOXYBENZOATE

56441-97-5

General method 1: 4-chloroquinazoline derivatives were synthesized as target products by the introduction of alkyl amino side chains. Specifically, this includes the preparation of 4-chloro-6-methoxy-7-[3-(4-methylpiperazin-1-yl)propoxy]quinazoline, 4-chloro-7-methoxy-6-[3-(4-methylpiperazin-1-yl)propoxy]quinazoline, and 4-chloro-6-methoxy-7-(3-pyrrolidin-1-ylpropoxy)quinazoline. Step 1: Methyl vanillate or methyl isovanillate (7.29 g, 40 mmol) was dissolved in 25 mL of dimethylformamide, followed by the addition of potassium carbonate (8.29 g, 60 mmol) and benzyl bromide (5.26 mL, 44 mmol). The reaction mixture was heated to 100 °C and maintained at this temperature for 3 hours. After completion of the reaction, it was cooled to room temperature, diluted with water and the product was extracted several times with ethyl acetate. The organic phases were combined and washed sequentially with water and brine. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent to obtain methyl 4-benzyloxy-3-methoxybenzoate or methyl 3-benzyloxy-4-methoxybenzoate, and the product could be used for subsequent reaction without further purification.

References[1] Patent: US2007/21446, 2007, A1. Location in patent: Page/Page column 14
[2] Patent: EP1785420, 2007, A1. Location in patent: Page/Page column 18
[3] Bioorganic and Medicinal Chemistry, 2009, vol. 17, # 18, p. 6728 - 6737
[4] Patent: EP1746096, 2007, A1. Location in patent: Page/Page column 23
[5] ChemMedChem, 2016, vol. 11, # 20, p. 2327 - 2338
Tag:METHYL 4-BENZYLOXY-3-METHOXYBENZOATE(56441-97-5) Related Product Information
Ethyl 4-(benzylaMino)butanoate hydrochloride METHYL 3,4,5-TRIS(BENZYLOXY)BENZOATE METHYL 7-METHOXY-2,2-DIPHENYL-1,3-BENZODIOXOLE-5-CARBOXYLATE METHYL 4-BENZYLOXY-3-METHOXYBENZOATE ETHYL 3,4-DIBENZYLOXYBENZOATE RARECHEM AL BI 0979 RARECHEM AL BF 1220 RARECHEM AL BF 0665 RARECHEM AL BI 1132 RARECHEM AL BI 1049 RARECHEM AL BF 1049 RARECHEM AL BI 1087 3,4,5-TRIBENZOYLOXYBENZOIC ACID N-PROPYL ESTER RARECHEM AL BF 1087 TOSLAB 12790 RARECHEM AL BI 0936 RARECHEM AL BF 1132 RARECHEM AL BF 0936

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