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ChemicalBook > Product Catalog >Pharmaceutical intermediates >Heterocyclic compound >Pyridine compound >Chloropyridine >4-Chloropyridine-3-carboxamide

4-Chloropyridine-3-carboxamide

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Products Intro: Product Name:4-Chloropyridine-3-carboxamide
CAS:7418-70-4
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Products Intro: Product Name:4-Chloropyridine-3-carboxamide
CAS:7418-70-4
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CAS:7418-70-4
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CAS:7418-70-4
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Products Intro: Product Name:4-Chloronicotinamide
CAS:7418-70-4
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4-Chloropyridine-3-carboxamide manufacturers
4-Chloropyridine-3-carboxamide Basic information
Product Name:4-Chloropyridine-3-carboxamide
Synonyms:4-Chloropyridine-3-carboxamide;4-Chloro-3-pyridinecarboxaMide;4-Chloropyridine-3-carboxamide ISO 9001：2015 REACH;3-Pyridinecarboxamide, 4-chloro-
CAS:7418-70-4
MF:C6H5ClN2O
MW:156.57
EINECS:
Product Categories:Pyridines
Mol File:7418-70-4.mol
4-Chloropyridine-3-carboxamide Structure
4-Chloropyridine-3-carboxamide Chemical Properties
Boiling point 299.5±25.0 °C(Predicted)
density 1.381±0.06 g/cm3(Predicted)
storage temp. Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka14.19±0.50(Predicted)
AppearanceLight yellow to yellow Solid
Safety Information
Hazard Codes Xn
Risk Statements 22
HS Code 2933399990
MSDS Information
4-Chloropyridine-3-carboxamide Usage And Synthesis
Synthesis
4-Chloronicotinic acid

10177-29-4

4-Chloropyridine-3-carboxamide

7418-70-4

Step A: Preparation of 4-chloronicotinamide: 4-chloronicotinic acid (10.00 g, 63.47 mmol) was mixed with SOCl2 (46.30 mL, 634.7 mmol) and heated and refluxed for 4 hours. Upon completion of the reaction, excess SOCl2 was removed by rotary evaporation. toluene (25 mL) was added to the residue and toluene was again removed by rotary evaporation. The resulting oily product was slowly poured into pre-cooled 25 mL of concentrated NH4OH (0 °C). After precipitating the solid, the product was collected by filtration to give 2.7 g of 4-chloronicotinamide in 27.6% yield.

References[1] Patent: US2007/49603, 2007, A1. Location in patent: Page/Page column 47
4-Chloropyridine-3-carboxamide Preparation Products And Raw materials
Raw materials4-Chloronicotinic acid-->Ammonia
Preparation Products4-Chloro-3-cyanopyridine
Tag:4-Chloropyridine-3-carboxamide(7418-70-4) Related Product Information
4,6-DICHLORO-NICOTINAMIDE N5-(3-CHLORO-4-FLUOROPHENYL)-4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE N5-(4-CHLOROPHENYL)-4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE N5-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE 4-CHLORO-N-(2,3-DIHYDRO-1H-INDEN-2-YL)-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE AURORA KA-5030 4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE N5-(2-CHLOROPHENYL)-4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE 2,4,5,6-TETRACHLORO-NICOTINAMIDE AURORA KA-6162 N3-(2,4-DICHLOROPHENYL)-4-CHLORONICOTINAMIDE N5-ISOPROPYL-4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE N-[(4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDIN-5-YL)CARBONYL]-N'-(4-FLUOROPHENYL)UREA 4-CHLORO-N-(2-HYDROXY-1,3-DIOXO-2,3-DIHYDRO-1H-INDEN-2-YL)-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDINE-5-CARBOXAMIDE AURORA KA-5031 AURORA KA-4988 5,7-DICHLORO-1,3,6-TRIPHENYL-1,2,3,4-TETRAHYDROPYRIDO[2,3-D]PYRIMIDINE-2,4-DIONE N-[(4-CHLORO-1,3-DIMETHYL-1H-PYRAZOLO[3,4-B]PYRIDIN-5-YL)CARBONYL]-N'-[3,5-DI(TRIFLUOROMETHYL)PHENYL]UREA
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