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4-AMINO-6-IODOPYRIMIDINE

4-AMINO-6-IODOPYRIMIDINE Suppliers list
Company Name: Accela ChemBio Inc.
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Email: info@accelachem.com
Products Intro: Product Name:4-Amino-6-iodopyrimidine
CAS:53557-69-0
Purity:>=97% Package:0.1g;0.25g;1g;5g;10g
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Products Intro: Product Name:6-Iodopyrimidin-4-amine
CAS:53557-69-0
Purity:97+% Package:1g;10g;100g;;1kg Remarks:Z-02295
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Products Intro: Product Name:4-AMINO-6-IODOPYRIMIDINE
CAS:53557-69-0
Purity:0.99 emma@coreychem.com Package:1000KG;100KG;1KG Emma
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Products Intro: Product Name:4-Amino-6-iodopyrimidine
CAS:53557-69-0
Purity:95% Package:$21.9/50mg;$36.9/100mg;$75.9/250mg;$228.9/1g;$971.9/5g;$1398.9/10g;Bulk package Remarks:95%
Company Name: Amadis Chemical Company Limited
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Products Intro: Product Name:6-Iodopyrimidin-4-amine
CAS:53557-69-0
Purity:0.97 Package:mgs,gs,kgs Remarks:A870694
4-AMINO-6-IODOPYRIMIDINE Basic information
Product Name:4-AMINO-6-IODOPYRIMIDINE
Synonyms:4-AMINO-6-IODOPYRIMIDINE;6-iodopyrimidin-4-ylamine;6-iodopyriMidin-4-aMine;6-iodo-4-Pyrimidinamine;4-Pyrimidinamine, 6-iodo-
CAS:53557-69-0
MF:C4H4IN3
MW:221
EINECS:
Product Categories:Heterocycle-Pyrimidine series
Mol File:53557-69-0.mol
4-AMINO-6-IODOPYRIMIDINE Structure
4-AMINO-6-IODOPYRIMIDINE Chemical Properties
Melting point 207-210 °C
Boiling point 345.0±27.0 °C(Predicted)
density 2.204±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
pka2.59±0.10(Predicted)
AppearanceLight yellow to light brown Solid
InChIInChI=1S/C4H4IN3/c5-3-1-4(6)8-2-7-3/h1-2H,(H2,6,7,8)
InChIKeyLQSJUQMCZHVKES-UHFFFAOYSA-N
SMILESC1=NC(I)=CC(N)=N1
Safety Information
MSDS Information
4-AMINO-6-IODOPYRIMIDINE Usage And Synthesis
Synthesis
4-Amino-6-chloropyrimidine

5305-59-9

4-AMINO-6-IODOPYRIMIDINE

53557-69-0

General procedure for the synthesis of 4-amino-6-iodopyrimidine from 4-amino-6-chloropyrimidine: a mixture of 4-amino-6-chloropyrimidine (1.00 g, 7.72 mmol), sodium iodide (5.79 g, 38.6 mmol) and 40% hydriodic acid (20 ml) was heated for 30 min at 70 °C. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove the precipitate. The filtrate was partitioned between dichloromethane and saturated sodium bicarbonate solution to separate the organic layer. The organic layer was dried with anhydrous sodium sulfate, filtered and the solvent evaporated to give 4-amino-6-iodopyrimidine (1.2 g, 70% yield). The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 6.89 (1H, s), 7.04 (2H, br s), 8.04 (1H, s).

References[1] Patent: WO2005/47279, 2005, A1. Location in patent: Page/Page column 50
[2] Patent: WO2005/60970, 2005, A1. Location in patent: Page/Page column 124
[3] European Journal of Medicinal Chemistry, 2014, vol. 80, p. 364 - 382
4-AMINO-6-IODOPYRIMIDINE Preparation Products And Raw materials
Raw materials4-Amino-6-chloropyrimidine-->Sodium iodide-->Hydriodic acid
Preparation Products5-bromo-6-iodopyrimidin-4-amine-->6-aminopyrimidine-4-carbonitrile
Tag:4-AMINO-6-IODOPYRIMIDINE(53557-69-0) Related Product Information
4-AMINO-6-IODO-2-METHYLPYRIMIDINE 4-AMINO-6-IODOPYRIMIDINE

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