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(R)-1-N-BOC-PIPECOLAMIDE

(R)-1-N-BOC-PIPECOLAMIDE Suppliers list
Company Name: Capot Chemical Co.,Ltd.
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Products Intro: Product Name:(R)-1-N-Boc-Piperidine-2-carboxamide
CAS:848488-91-5
Purity:98%(Min,HPLC) Package:100g;1kg;5kg,10kg,25kg,50kg
Company Name: Alchem Pharmtech,Inc.
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Products Intro: Product Name:N-Boc-D-2-Piperidinecarboxamide
CAS:848488-91-5
Purity:97+% Package:1g;10g;100g;;1kg Remarks:Z-21194
Company Name: CONIER CHEM AND PHARMA LIMITED
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Products Intro: Product Name:n-boc-d-2-piperidinecarboxamide
CAS:848488-91-5
Purity:0.99 Package:1kg
Company Name: Blocksynth Pharmaceutical Technology Co.,Ltd
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Products Intro: Product Name:(R)-1-N-BOC-PIPECOLAMIDE
CAS:848488-91-5
Purity:99% Package:20KG;USD
Company Name: AFINE CHEMICALS LIMITED
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Products Intro: Product Name:(R)-1-N-BOC-PIPECOLAMIDE
CAS:848488-91-5
Purity:98%+ Package:Standard or custom package Remarks:excellent quality and reliable supplier
(R)-1-N-BOC-PIPECOLAMIDE Basic information
Product Name:(R)-1-N-BOC-PIPECOLAMIDE
Synonyms:N-Boc-D-2-piperidinecarboxamide;(R)-2-Carbamoyl-piperidine-1-carboxylic acid tert-butyl ester;(R)-tert-butyl 2-carbamoylpiperidine-1-carboxylate;1-Piperidinecarboxylic acid, 2-(aminocarbonyl)-, 1,1-dimethylethyl ester, (2R)-;(R)-tert-Butyl 2-carbamoyllpiperidine-1-carboxylate;(R)-1-Boc-2-piperidinecarboxaMide;(R)-1-Boc-2-(aminocarbonyl)piperidine;tert-Butyl (R)-2-carbamoylpiperidine-1-carboxylate
CAS:848488-91-5
MF:C11H20N2O3
MW:228.29
EINECS:
Product Categories:
Mol File:848488-91-5.mol
(R)-1-N-BOC-PIPECOLAMIDE
 Structure
(R)-1-N-BOC-PIPECOLAMIDE Chemical Properties
storage temp. Sealed in dry,Room Temperature
AppearanceWhite to off-white Solid
Safety Information
MSDS Information
(R)-1-N-BOC-PIPECOLAMIDE Usage And Synthesis
Synthesis
(R)-(+)-N-Boc-2-piperidinecarboxylic acid

28697-17-8

(R)-1-N-BOC-PIPECOLAMIDE

848488-91-5

Step B. Synthesis of tert-butyl (2R)-2-(aminocarbonyl)piperidine-1-carboxylate: To a mixture of (2R)-1-(tert-butoxycarbonyl)piperidine-2-carboxylic acid (2.29 g, 10 mmol), ammonium chloride (3.21 g, 60 mmol), and DMF (70 mL) was added HATU (5.60 g, 14.7 mmol) at 0 °C and DIPEA (3.88 g, 30 mmol). The reaction mixture was stirred at room temperature for 18 hours. After completion of the reaction, the reaction solution was diluted with H2O (100 mL) and extracted with EtOAc (3 x 100 mL). The organic phases were combined and washed sequentially with 10% Na2CO3 solution (2 × 30 mL), brine (2 × 30 mL) and then dried with Na2SO4. After filtration and concentration, it was purified by MPLC on silica gel using hexane/EtOAc (1:1) as eluent to afford R-N-Boc-prolinamide as a white solid.1H NMR (400 MHz, CDCl3) δ: 1.46 (s, 9H), 1.63 (m, 2H), 2.22 (m, 1H), 2.91 (m, 1H), 3.06 (m, 3H), 4.01 (m, 1H), 4.71 (m, 1H), 6.46 (br, 2H).MS (ESI) m/z: 228.92 (M+H)+.

References[1] Patent: WO2005/115986, 2005, A1. Location in patent: Page/Page column 103
[2] Patent: WO2006/116764, 2006, A1. Location in patent: Page/Page column 121; 151
[3] Patent: US2008/300279, 2008, A1. Location in patent: Page/Page column 9
[4] ACS Infectious Diseases, 2018, vol. 4, # 7, p. 1130 - 1145
(R)-1-N-BOC-PIPECOLAMIDE Preparation Products And Raw materials
Raw materials(R)-(+)-N-Boc-2-piperidinecarboxylic acid-->HATU-->N,N-Diisopropylethylamine-->N,N-Dimethylformamide-->Ammonium chloride
Tag:(R)-1-N-BOC-PIPECOLAMIDE (848488-91-5) Related Product Information
2-(2-HYDROXY-ETHYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER (R)-N-Boc-glutamic acid-1,5-dimethyl ester Pipecolamide (+/-)-1-N-BOC-PIPERIDINE-2-CARBOXAMIDE (R)-1-N-BOC-PIPECOLAMIDE 2-(Boc-aminomethyl)-piperidine (R)-2-AMINOMETHYL-1-N-BOC-PIPERIDINE (R)-2-FORMYL-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER (S)-(+)-N-TBOC-2-METHYLPIPERIDINE

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