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4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID

4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID Struktur
245349-46-6
CAS-Nr.
245349-46-6
Englisch Name:
4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID
Synonyma:
4-(3-(acryloyloxy)propoxy)benzoic acid;4-(3-prop-2-enoyloxypropoxy)benzoic acid;4-(3-(acryloyloxy)propyloxy)benzoic acid;4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID;Benzoic acid,4-[3-[(1-oxo-2-propen-1-yl)oxy]propoxy]-
CBNumber:
CB61512524
Summenformel:
C13H14O5
Molgewicht:
250.25
MOL-Datei:
245349-46-6.mol

4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID Eigenschaften

Siedepunkt:
428.1±25.0 °C(Predicted)
Dichte
1.208±0.06 g/cm3(Predicted)
storage temp. 
2-8°C, stored under nitrogen
pka
4.44±0.10(Predicted)
Aussehen
White to off-white Solid
InChI
InChI=1S/C13H14O5/c1-2-12(14)18-9-3-8-17-11-6-4-10(5-7-11)13(15)16/h2,4-7H,1,3,8-9H2,(H,15,16)
InChIKey
AHBWYWGJQFTBRO-UHFFFAOYSA-N
SMILES
C(O)(=O)C1=CC=C(OCCCOC(=O)C=C)C=C1

Sicherheit

4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID Chemische Eigenschaften,Einsatz,Produktion Methoden

synthetische

The preparation of 4-(3-acryloyloxy-n-prop-1-yloxy)benzoic acid is as follows:8.1g Allyl 4- (3- (acryloyloxy) propoxy) benzoic acid,4.1 g of N-methylaniline,Add 0.28 g of palladium acetate and 0.66 g of triphenylphosphine to 50 mL of acetonitrile, andStir at room temperature overnight. The reaction solution is diluted with ethyl acetate,The extract was washed with 5% hydrochloric acid and saturated brine, dried over anhydrous sodium sulfate, the solid was filtered off, and the solvent was evaporated. The residue is purified by column chromatography (silica gel, developing solvent: dichloromethane) to yield 4.2 g of 4- (3- (Acryloyloxy) propoxy) benzoic acid(Yield: 80.0%, purity (HPLC): 93.0%) was obtained.

245349-46-6.png

4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene

4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 56)Lieferanten
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245349-46-6()Verwandte Suche:

  • 4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID
  • 4-(3-(acryloyloxy)propyloxy)benzoic acid
  • 4-(3-prop-2-enoyloxypropoxy)benzoic acid
  • Benzoic acid,4-[3-[(1-oxo-2-propen-1-yl)oxy]propoxy]-
  • 4-(3-(acryloyloxy)propoxy)benzoic acid
  • 245349-46-6
  • API intermediates
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