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2-[2-(2-Azidoethoxy)ethoxy]ethanamine

2-[2-(2-Azidoethoxy)ethoxy]ethanamine Struktur
166388-57-4
CAS-Nr.
166388-57-4
Englisch Name:
2-[2-(2-Azidoethoxy)ethoxy]ethanamine
Synonyma:
N3-PEG2-NH2;Azido-PEG2-NH2;H2N-C2-PEG2-N3;Azide-PEG3-Amine;Azido-PEG2-Amine;N3-PEG2-CH2CH2NH2;Azido-PEG2-C2-amine;Azido-PEG2-CH2CH2NH2;Azido-PEG2-CH2CH2-Amine;Amino-PEG2-azide,NH2-PEG2-N3
CBNumber:
CB02484811
Summenformel:
C6H14N4O2
Molgewicht:
174.2
MOL-Datei:
166388-57-4.mol

2-[2-(2-Azidoethoxy)ethoxy]ethanamine Eigenschaften

storage temp. 
-20°C, protect from light
L?slichkeit
Soluble in Water, DMSO, DMF, DCM
Aggregatzustand
Liquid
Farbe
Colorless to light yellow
InChI
InChI=1S/C6H14N4O2/c7-1-3-11-5-6-12-4-2-9-10-8/h1-7H2
InChIKey
ZHWGWSYNZIZTFL-UHFFFAOYSA-N
SMILES
NCCOCCOCCN=[N+]=[N-]
CAS Datenbank
166388-57-4
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
HS Code  2929900090
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Achtung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H314 Verursacht schwere Ver?tzungen der Haut und schwere Augensch?den. ?tzwirkung auf die Haut Kategorie 1B Achtung GHS hazard pictogramssrc="/GHS05.jpg" width="20" height="20" /> P260,P264, P280, P301+P330+ P331,P303+P361+P353, P363, P304+P340,P310, P321, P305+ P351+P338, P405,P501
Sicherheit
P260 Dampf/Aerosol/Nebel nicht einatmen.
P280 Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.

2-[2-(2-Azidoethoxy)ethoxy]ethanamine Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

2-[2-(2-Hydroxyethoxy)ethoxy]ethyl chloride (15 g, 88.9 mmol), NaI(4.06 g, 27.1 mmol), and NaN3 (45.3 mg, 697 mmol) were dissolved in distilled water (90 mL), and the solution was stirred for 48 h at 50 °C. The reaction mixture extracted with ethyl acetate for three times. The organic layer was dried over Na2SO4 , and evaporated to collect 2-[2-(2-azidoethoxy)ethoxy]ethanol (14.0 g, 90.1%) as a yellow oil.To the solution 2-[2-(2-azidoethoxy)ethoxy]ethanol (8 g, 45.7 mmol) in THF (22.4 mL), 6 M NaOH(20.8 mL) and TsCl (13.1 g, 68.6 mmol) were added at 0 °C. The reaction mixture was stirred for 1 h at room temperature under nitrogen atmosphere. The solution was then extracted with diethyl ether four times, and the organic layer was washed with 1 M NaOH. After evaporation of the organic layer,2-[2-(2-azidoethoxy)ethoxy]ethyl tosylate (16.8 g, 98.6%) was obtained as a yellow oil.Finally, ammonia solution (28%, 14.8 mL, 365 mol) was added to the 2-[2-(2-azidoethoxy)ethoxy]-ethyl tosylate (8 g, 24.3 mmol) dissolved in THF (95.9 mL), and reaction mixture was stirred for 96 h at 40 °C. After the reaction, distilled water (50 mL) was added to the solution. The mixture was washed with diethyl ether and then extracted with dichloromethane. The organic layer was dried over NaSO4 and evaporated to obtain 2-[2-(2-azidoethoxy)ethoxy]ethanamine (2.49 g, 58.8%) as a yellow oil.
synthesis of 2-[2-(2-Azidoethoxy)ethoxy]ethanamine

2-[2-(2-Azidoethoxy)ethoxy]ethanamine Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


2-[2-(2-Azidoethoxy)ethoxy]ethanamine Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 120)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795
ivan@atkchemical.com China 33024 60
Accela ChemBio Inc.
+1-858-6993322
info@accelachem.com United States 21193 58
CONIER CHEM AND PHARMA LIMITED
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SHANGHAI T&W PHARMACEUTICAL CO., LTD.
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contact@trustwe.com China 5745 58
Zhengzhou Alfa Chemical Co.,Ltd
+8618530059196
sale04@alfachem.cn China 12434 58
TargetMol Chemicals Inc.
+1-781-999-5354; +17819995354
marketing@targetmol.com United States 32376 58
Wuhan Borenpharm Co., Ltd
027-65563561 18717150066
3207347307@qq.com CHINA 1238 58
Shanxi Xuanran Import and Export Trade Co., Ltd.
+8617735180244
mike_yan@xuanranglobal.com CHINA 4017 58
Nextpeptide Inc
+86-0571-81612335 +8613336028439
sales@nextpeptide.com China 19908 58
InvivoChem
+1-708-310-1919 +1-13798911105
sales@invivochem.cn United States 6391 58

166388-57-4()Verwandte Suche:


  • N3-PEG2-CH2CH2NH2
  • Azido-PEG2-Amine
  • 2-[2-(2-Azidoethoxy)ethoxy]ethanamine
  • N3-PEG2-NH2
  • Azido-PEG2-NH2
  • 2-[2-(2-Azido-ethoxy)-ethoxy]-ethylamine
  • Azido-PEG2-C2-amine
  • Amino-PEG2-azide,NH2-PEG2-N3
  • Azide-PEG3-Amine
  • Ethanamine, 2-[2-(2-azidoethoxy)ethoxy]-
  • N3-PEG2-CH2CH2NH2/Ethanamine, 2-[2-(2-azidoethoxy)ethoxy]-
  • H2N-C2-PEG2-N3
  • Azido-PEG2-CH2CH2NH2
  • Azido-PEG2-CH2CH2-Amine
  • 166388-57-4
  • 1660388-57-4
  • peg
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