Identification | More | [Name]
4-HYDROXY-8-METHYLQUINOLINE-3-CARBOXYLIC ACID ETHYL ESTER | [CAS]
77156-75-3 | [Synonyms]
4-HYDROXY-8-METHYLQUINOLINE-3-CARBOXYLIC ETHYL 4-HYDROXY-8-METHYL-3-QUINOLINECARBOXYLATE ETHYL 4-HYDROXY-8-METHYLQUINOLINE-3-CARBOXYLATE Ethyl 8-methyl-4-oxo-1H-quinoline-3-carboxylate 2-ethyl-8-methyl-4-oxo-1H-quinoline-3-carboxylate 4-HYDROXY-8-METHYLQUINOLINE-3-CARBOXYLIC ETHYL ESTER 4-HYDROXY-8-METHYLQUINOLINE-3-CARBOXYLIC ACID ETHYL ESTER 3-Quinolinecarboxylic acid, 4-hydroxy-8-methyl-, ethyl ester | [Molecular Formula]
C13H13NO3 | [MDL Number]
MFCD00173390 | [Molecular Weight]
231.25 | [MOL File]
77156-75-3.mol |
Hazard Information | Back Directory | [Synthesis]
GENERAL METHOD: 2e-k (4 mmol) was dissolved in diphenyl ether with a catalytic amount of 2-chlorobenzoic acid and heated by microwave radiation at 250°C for 1-2 hours. After completion of the reaction, the reaction mixture was cooled, the precipitate 3e-k was collected by filtration and washed sequentially with hexane and water. | [References]
[1] Journal of Heterocyclic Chemistry, 2013, vol. 50, # SUPPL.1, p. E1-E8 [2] Nucleosides and Nucleotides, 1996, vol. 15, # 4, p. 889 - 898 [3] Medicinal Chemistry Research, 2016, vol. 25, # 9, p. 1861 - 1876 [4] Journal of Medicinal Chemistry, 2006, vol. 49, # 22, p. 6443 - 6450 [5] RSC Advances, 2014, vol. 4, # 12, p. 6254 - 6260 |
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Energy Chemical
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