(R)-2-methyl-1-phenylpropan-1-amine hydrochloride synthesis
- Product Name:(R)-2-methyl-1-phenylpropan-1-amine hydrochloride
- CAS Number:51600-25-0
- Molecular formula:C10H16ClN
- Molecular Weight:185.6937
108-86-1
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![2-Propanesulfinamide, 2-methyl-N-(2-methylpropylidene)-, [S(S)]-](/CAS/20210305/GIF/1175603-96-9.gif)
1175603-96-9
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51600-25-0
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$161.00/250mg
Yield:51600-25-0 80.1%
Reaction Conditions:
Stage #1: bromobenzenewith n-butyllithium in tetrahydrofuran;hexane at -50 - -40;
Stage #2: Ss-2-methyl-propane-2-sulfinic acid [2-methylpropylidene]amide in tetrahydrofuran;hexane at -50 - -40;
Stage #3: with hydrogenchloride in isopropyl alcohol; for 1 h;enantioselective reaction;
References:
Rajendiran, Chinnapillai;Nagarajan, Periyandi;Naidu;Dubey [Synthetic Communications,2014,vol. 44,# 20,p. 2936 - 2942]
186249-76-3
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51600-25-0
42 suppliers
$161.00/250mg