QUINAZOLIN-4-YLAMINE synthesis
- Product Name:QUINAZOLIN-4-YLAMINE
- CAS Number:15018-66-3
- Molecular formula:C8H7N3
- Molecular Weight:145.16
1227920-69-5
15018-66-3
General method: Method B: The formimide or acetimide amide intermediate was suspended in a mixture of formamide (40 eq.) and InCl3 (1 eq.) in a sealed vial. Subsequently, the reaction was irradiated in a microwave reactor at 400 W power. After completion of the reaction, the reaction mixture was cooled to room temperature, the solid product was collected by filtration, washed with water and finally dried to give quinolin-4-amine.
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15018-66-3
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Yield: 77%
Reaction Conditions:
with formamide at 200; for 0.166667 h;Microwave irradiation;Sealed vial;
Steps:
4.3. General procedures for the syntheses of quinazolin4-amines
General procedure: Method B: Formimidamide or acetimidamide intermediates were suspended in formamide (40 equiv) and InCl3 (1 equiv), or not, in a sealed vial and were irradiated at 400 W under microwaves. The residue was cooled to room temperature, filtrated, washed with water and dried.
References:
Loidreau, Yvonnick;Besson, Thierry [Tetrahedron,2011,vol. 67,# 26,p. 4852 - 4857] Location in patent:experimental part
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15018-66-3
110 suppliers
$22.00/250mg