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ChemicalBook CAS DataBase List Buparlisib Hydrochloride
1312445-63-8

Buparlisib Hydrochloride synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium acetate / tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium(0) / 2 h / 84 °C / Inert atmosphere
2: caesium carbonate / dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II) / water; tetrahydrofuran / 0.75 h / 45 °C / Inert atmosphere
3: hydrogenchloride / isopropyl alcohol; acetone / 2.25 h / Inert atmosphere

References:

WO2012/44727,2012,A2

106447-97-6 Synthesis
2-Amino-4-(trifluoromethyl)pyridine

106447-97-6
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Buparlisib Hydrochloride

1312445-63-8
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