N-Vinylcaprolactam synthesis
- Product Name:N-Vinylcaprolactam
- CAS Number:2235-00-9
- Molecular formula:C8H13NO
- Molecular Weight:139.19
13344-00-8
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2235-00-9
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Yield:2235-00-9 81.9%
Steps:
2 Inventive
Example 2 Inventive Example 2 was carried out by adding 1% by weight of 1,4-diethoxybutane as cocatalyst. The amount of ethyne taken up was 0.87 mol per mole of ε-caprolactam. The distillative workup yielded N-vinyl-ε-caprolactam in a yield of 81.9%. A liquid distillation residue was obtained.
References:
US2003/28035,2003,A1
105-60-2
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2235-00-9
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2235-00-9
294 suppliers
$5.00/5g