N-Methyl-1-amino-hex-5-ene synthesis
- Product Name:N-Methyl-1-amino-hex-5-ene
- CAS Number:55863-02-0
- Molecular formula:C7H15N
- Molecular Weight:113.2
2695-47-8
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74-89-5
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55863-02-0
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Yield:55863-02-0 67%
Reaction Conditions:
in methanol at 40; for 3 h;Solvent;Temperature;
Steps:
9 Example 9: A synthesis process of N-methyl-5-hexen-1-amine, which differs from Example 1 in that it includes
The following steps: adding 25% methylamine in methanol to the reaction flask, the methylamine content is 10 equivalents,Add 1 equivalent of 6-bromo-1-hexene to the reaction flask, stir, and heat the oil bath to 40° C. After 3 hours of reaction, cool down to 20° C. and add 0.1 equivalent of stable.Stabilizer, stabilizing agent is p-methoxy phenol, 1 equivalent of sodium hydroxide is added, excess methylamine methanol solution is recovered under negative pressure, heated to 50°C,Distillation under reduced pressure gave a colorless liquid, which was N-methyl-5-hexen-1-amine, with a yield of 67% and a purity of 96.5%.
References:
CN108003037,2018,A Location in patent:Paragraph 0014-0028
922520-05-6
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55863-02-0
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34825-70-2
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55863-02-0
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50347-17-6
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55863-02-0
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821-41-0
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55863-02-0
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