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ChemicalBook CAS DataBase List METHYL 1-METHYLPYRROLE-2-CARBOXYLATE
37619-24-2

METHYL 1-METHYLPYRROLE-2-CARBOXYLATE synthesis

13synthesis methods
-

Yield:-

Reaction Conditions:

at 20; for 1 h;

Steps:

26
To a solution of 1-methyl-2-pyrrolecarboxylic acid (1.03 g, 8.22 mmol) in MeOH (5 mL) and dioxane (5 mL) at room temperature, trimethylsilyldiazomethane (2M in ether, 5.0 mL, 10.0 mmol) was added. After being stirred at room temperature for 1 h, the mixture was concentrated in vacuo to give methyl 1-methyl-2-pyrrolecarboxylate as a volatile oil (1.14 g).

References:

Millennium Pharmaceuticals, Inc. US2007/259924, 2007, A1 Location in patent:Page/Page column 33

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