ETHYLENE DI(THIOTOSYLATE) synthesis
- Product Name:ETHYLENE DI(THIOTOSYLATE)
- CAS Number:2225-23-2
- Molecular formula:C16H18O4S4
- Molecular Weight:402.57
824-79-3
419 suppliers
$6.00/25g
106-93-4
409 suppliers
$15.00/5g
2225-23-2
43 suppliers
$60.00/100mg
Yield:2225-23-2 98%
Reaction Conditions:
Stage #1: sodium 4-methylbenzenesulfinatewith pyridine;sulfur for 48 h;
Stage #2: in water at 20; for 18 h;
Stage #3: ethylene dibromide in toluene; for 20 h;Heating;Further stages.;
References:
Deguest, Geoffrey;Bischoff, Laurent;Fruit, Corinne;Marsais, Francis [Synthetic Communications,2008,vol. 38,# 6,p. 841 - 847]
