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ChemicalBook CAS DataBase List DIISOPROPYLCARBAMOYL CHLORIDE
19009-39-3

DIISOPROPYLCARBAMOYL CHLORIDE synthesis

6synthesis methods
-

Yield: 88.65%

Reaction Conditions:

Stage #1:tetraisopropylothiuram disulphide with chlorine in dichloromethane at 24 - 26; for 7.16667 h;Cooling with ice;
Stage #2: with water;sodium hydrogencarbonate in dichloromethaneCooling with ice;

References:

Adeppa;Rupainwar;Misra, Krishna [Synthetic Communications,2011,vol. 41,# 2,p. 285 - 290] Location in patent:experimental part

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