Diaminomaleonitrile synthesis
- Product Name:Diaminomaleonitrile
- CAS Number:1187-42-4
- Molecular formula:C4H4N4
- Molecular Weight:108.1
75-86-5
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1187-42-4
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Yield:1187-42-4 88%
Reaction Conditions:
with sodium cyanide;methylthiol at 60; for 2 h;Autoclave;Temperature;Time;Reagent/catalyst;
Steps:
2
Example 2 In an autoclave, 10 g of NaCN is added to 130 ml of acetone cyanohydrin. Then 6.54 g of methanethiol is added. The solution is then stirred at 60° C. for 2 hours. The solution turns orange. The excess acetone cyanohydrin is then neutralized by adding soda. The solution is then filtered and evaporated to give an orange-yellow solid (amount recovered=33.7 g corresponding to a yield=88%).
References:
US2015/197487,2015,A1 Location in patent:Paragraph 0029
![Methanimidic acid, N-[(1Z)-2-amino-1,2-dicyanoethenyl]-, ethyl ester, (Z)-](/CAS/20200611/GIF/129694-52-6.gif)
129694-52-6
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619-45-4
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![METHYL 4-[(([(Z)-2-AMINO-1,2-DICYANOETHENYL]IMINO)METHYL)AMINO]BENZENECARBOXYLATE](/StructureFile/ChemBookStructure4/GIF/CB4287670.gif)
931424-12-3
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1187-42-4
343 suppliers
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74-90-8
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1187-42-4
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