Decanoyl chloride synthesis
- Product Name:Decanoyl chloride
- CAS Number:112-13-0
- Molecular formula:C10H19ClO
- Molecular Weight:190.71
334-48-5
651 suppliers
$6.00/25g
112-13-0
290 suppliers
$14.00/25g
Yield:112-13-0 100%
Reaction Conditions:
with oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 0 - 20; for 4 h;
Steps:
a a) Decanoyl chloride
To a cooled (0 °C) solution of decanoic acid (275 mg, 1.59 mmol) in DCM (8 mL) was added dropwise oxalyl chloride (0.56 mL, 6.39 mmol) and DMF (3 drops) and the mixture was stirred at room temperature for 4 h. The solvent was removed under reduced pressure to yield the title compound as a yellow oil (315 mg, 100%) which was used in the next synthetic step without further purification.
References:
ALMIRALL, S.A.;BACH TA?A, Jordi;ESTEVE TRIAS, Cristina;MIR CEPEDA, Marta WO2019/115405, 2019, A1 Location in patent:Page/Page column 48
142-62-1
480 suppliers
$13.80/2.5g
112-13-0
290 suppliers
$14.00/25g
108-31-6
878 suppliers
$13.47/50 G
60-32-2
615 suppliers
$5.00/10g
112-13-0
290 suppliers
$14.00/25g
79-37-8
489 suppliers
$17.67/10gm:
334-48-5
651 suppliers
$6.00/25g
112-13-0
290 suppliers
$14.00/25g
111-66-0
173 suppliers
$10.00/10 mL
112-13-0
290 suppliers
$14.00/25g