Benzeneacetic acid, 2-chloro-5-methyl-4-nitro- synthesis

1synthesis methods

Product Name:Benzeneacetic acid, 2-chloro-5-methyl-4-nitro-
CAS Number:1428761-24-3
Molecular formula:C9H8ClNO4
Molecular Weight:229.62

57310-39-1 Synthesis

57310-39-1
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Benzeneacetic acid, 2-chloro-5-methyl-4-nitro-

1428761-24-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: sulfuric acid; nitric acid / 3 h / 0 - 5 °C
2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 16 h / 90 °C
3: sodium periodate; ruthenium(III) chloride monohydrate; tetra-(n-butyl)ammonium iodide / water; ethyl acetate / 0 - 20 °C

References:

WO2013/43232,2013,A2

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Benzeneacetic acid, 2-chloro-5-methyl-4-nitro- synthesis