(αS,βS)-β-[(2-AMinophenyl)thio]-α-hydroxy-4-Methoxybenzenepropanoic Acid Methyl Ester synthesis
- Product Name:(αS,βS)-β-[(2-AMinophenyl)thio]-α-hydroxy-4-Methoxybenzenepropanoic Acid Methyl Ester
- CAS Number:99109-07-6
- Molecular formula:C17H19NO4S
- Molecular Weight:333.4
105560-93-8
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99109-07-6
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Yield:-
Reaction Conditions:
in toluene;
Steps:
2 EXAMPLE 2
EXAMPLE 2 A mixture of 40 g of methyl (2R,3S)-2,3-epoxy-3-(4-methoxyphenyl)propionate, 26.5 g of 2-aminothiophenol and 300 ml of toluene is heated at 110° to 115° C. for 1 hour, whereby the reaction mixture containing methyl (2S,3S)-3-[(2-aminophenyl)thio]-2-hydroxy-3-(4-methoxylphenyl)propionate is obtained.
References:
US5294706,1994,A
4875-10-9
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99109-07-6
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$165.00/10mg