ChemicalBook CAS DataBase List 7-Iodo Sancycline

7-Iodo Sancycline synthesis

2synthesis methods

Product Name:7-Iodo Sancycline
CAS Number:113164-67-3
Molecular formula:C21H21IN2O7
Molecular Weight:540.31

64-73-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: triethylamine; palladium on activated charcoal; hydrogen / ethanol
2: rhodium contaminated with carbon; hydrogen; toluene-4-sulfonic acid / methanol / -5 - 5 °C
3: sulfuric acid; N-iodo-succinimide / 2 h / 0 - 10 °C

References:

CN106831479,2017,A

987-02-0
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References

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7-Iodo Sancycline synthesis