6-methyl-2-phenyl-1H-indole synthesis
- Product Name:6-methyl-2-phenyl-1H-indole
- CAS Number:66354-87-8
- Molecular formula:C15H13N
- Molecular Weight:207.27
1037493-10-9
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66354-87-8
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Yield:66354-87-8 98%
Reaction Conditions:
with silver nitrate in water at 130;Sealed tube;Sonication;Green chemistry;regioselective reaction;
Steps:
2-Phenyl-1H-pyrrolo[2,3-b]pyridine (2a); Typical Procedure
General procedure: To a sealed tube (10 mL) was added 3-(phenylethynyl)pyridin-2-amine (1a; 50 mg, 0.26 mmol), H2O (2 mL), and AgNO3 (8.7 mg, 0.052 mmol). After ultrasonic oscillation for 5 min, the mixture was stirred at 130 °C for about 16 h. The reaction product was filtered, washed with H2O, and dried to give a brown solid; yield: 48 mg (96%); mp 209-210 °C; HPLC purity 98%.
References:
Sun, Hongpeng;Xiao, Li;Li, Wei;Xie, Qiong;Shao, Liming [Synthesis,2017,vol. 49,# 21,p. 4845 - 4852] Location in patent:supporting information
1037492-69-5
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66354-87-8
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![Benzene, 2-azido-4-methyl-1-[(1E)-2-phenylethenyl]-](/CAS/20211123/GIF/1054566-90-3.gif)
1054566-90-3
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