5-PHENYL-1,3,4-OXADIAZOLE-2-CARBONYL CHLORIDE synthesis
- Product Name:5-PHENYL-1,3,4-OXADIAZOLE-2-CARBONYL CHLORIDE
- CAS Number:98591-60-7
- Molecular formula:C9H5ClN2O2
- Molecular Weight:208.6
99066-76-9
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$125.00/500mg
98591-60-7
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$24.00/100mg
Yield:-
Reaction Conditions:
with thionyl chloride for 4 h;Reflux;
Steps:
4.3 5-Phenyl-1,3,4-oxadiazole-2-carbonyl chloride (5)
5-Phenyl-1,3,4-oxadiazole-2-carboxylic acid (4) (400 mg, 2.11 mmol) was dissolved in thionyl chloride (4mL) and refluxed for four hours. Then the mixture was concentrated in vacuum and used without any purification.
References:
Polyak, Maria;Varga, Gergely;Szilagyi, Bence;Juhasz, Laszlo;Docsa, Tibor;Gergely, Pal;Begum, Jaida;Hayes, Joseph M.;Somsak, Laszlo [Bioorganic and Medicinal Chemistry,2013,vol. 21,# 18,p. 5738 - 5747]
613-94-5
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98591-60-7
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16691-25-1
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60214-04-2
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98591-60-7
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79-37-8
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18039-42-4
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98591-60-7
25 suppliers
$24.00/100mg