4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE synthesis
- Product Name:4-(2-METHOXYPHENYL)-2-METHYL-1-BUTENE
- CAS Number:18272-85-0
- Molecular formula:C12H16O
- Molecular Weight:176.25
Yield:18272-85-0 89%
Reaction Conditions:
Stage #1: Methyltriphenylphosphonium bromidewith sodium t-butanolate in tetrahydrofuran at 0; for 0.5 h;
Stage #2: 4-(o-methoxyphenyl)-butan-2-one in tetrahydrofuran at 20; for 3 h;
References:
Lu, Yanhui;Nakatsuji, Hidefumi;Okumura, Yukimasa;Yao, Lu;Ishihara, Kazuaki [Journal of the American Chemical Society,2018,vol. 140,# 19,p. 6039 - 6043] Location in patent:supporting information
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