2-Isopropylphenol synthesis
- Product Name:2-Isopropylphenol
- CAS Number:88-69-7
- Molecular formula:C9H12O
- Molecular Weight:136.19
89787-12-2
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88-69-7
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$5.00/5 g
Yield:88-69-7 90%
Reaction Conditions:
with iron(III) oxide;oxygen in tetrahydrofuranIrradiation;
Steps:
General procedure for the preparation of phenols from arylboronic acids:
General procedure: In atypical procedure, a flask containing phenylboronic acid (100 mg, 0.82 mmol) was taken and to it were added 10 mol % of iron(III) oxide photocatalyst(13.1 mg) and tetrahydrofuran (2 ml). The reaction mixture was kept for stirring under diffused sunlight in ordinary open flask until the starting material is consumed on TLC. Quenched with water after completion and the catalyst was filtered off, the filtrate was concentrated in vacuo. The crudeproduct was purified on silica (100-200 mesh) column chromatography (15%ethylacetate/hexane) to offer 73.2 mg (in 95% yield) of pure crystalline phenol.
References:
Sawant, Sanghapal D.;Hudwekar, Abhinandan D.;Aravinda Kumar;Venkateswarlu, Vunnam;Singh, Parvinder Pal;Vishwakarma, Ram A. [Tetrahedron Letters,2014,vol. 55,# 4,p. 811 - 814]
7073-94-1
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88-69-7
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2944-47-0
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$12.00/5g
88-69-7
192 suppliers
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67-63-0
1612 suppliers
$16.00/25ML
108-95-2
764 suppliers
$14.00/25g
88-69-7
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99-89-8
202 suppliers
$13.00/10g
2078-54-8
417 suppliers
$24.69/25g
2934-07-8
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inquiry
67-63-0
1612 suppliers
$16.00/25ML
108-95-2
764 suppliers
$14.00/25g
88-69-7
192 suppliers
$5.00/5 g
99-89-8
202 suppliers
$13.00/10g
2078-54-8
417 suppliers
$24.69/25g
2741-16-4
87 suppliers
$9.00/1g