2-Iodoazulene synthesis
- Product Name:2-Iodoazulene
- CAS Number:36044-41-4
- Molecular formula:C10H7I
- Molecular Weight:254.07
3839-48-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: ethanol; sodium / 72.15 h / 20 °C
2: lithium chloride / N,N-dimethyl-formamide; water / 21 h / Reflux
3: phosphorus tribromide / toluene / 2 h / 90 °C / Inert atmosphere
4: copper(l) iodide; potassium iodide / N,N-dimethyl-formamide / 16 h / Reflux
References:
Ohtsu, Keito;Hayami, Ryohei;Sagawa, Takuya;Tsukada, Satoru;Yamamoto, Kazuki;Gunji, Takahiro [Tetrahedron,2019,vol. 75,# 46,art. no. 130658]
58312-57-5
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457644-50-7
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19384-00-0
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36044-40-3
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