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20041-61-6

2-HYDROXY-3-METHOXY-4-NITROBENZALDEHYDE synthesis

6synthesis methods
7150-01-8 Synthesis
2-ACETOXY-3-METHOXYBENZALDEHYDE 97

7150-01-8
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Yield:20041-61-6 57%

Reaction Conditions:

Stage #1: 2-acetoxy-3-methoxybenzaldehydewith sulfuric acid;nitric acid at -40; for 0.0833333 h;
Stage #2: with sodium hydroxide in methanol;water at 85; for 2 h;

References:

JP2015/166329,2015,A Location in patent:Paragraph 0074-0075