2-(Di-tert-butylphosphino)-2',6'-dimethoxybiphenyl synthesis
- Product Name:2-(Di-tert-butylphosphino)-2',6'-dimethoxybiphenyl
- CAS Number:819867-21-5
- Molecular formula:C22H31O2P
- Molecular Weight:358.45
694-80-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 1.75 h / 0 - 20 °C
1.2: 0.5 h / 0 °C
2.1: magnesium; ethylene dibromide / tetrahydrofuran / 1 h / 80 °C / Inert atmosphere
2.2: 18 h / 20 °C
References:
Golding, William A.;Pearce-Higgins, Robert;Phipps, Robert J. [Journal of the American Chemical Society,2018,vol. 140,# 42,p. 13570 - 13574]
819-19-2
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755017-61-9
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151-10-0
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