ChemicalBook CAS DataBase List 2-BROMO-5-METHYL-1-BENZOTHIOPHENE

2-BROMO-5-METHYL-1-BENZOTHIOPHENE synthesis

1synthesis methods

Product Name:2-BROMO-5-METHYL-1-BENZOTHIOPHENE
CAS Number:111860-00-5
Molecular formula:C9H7BrS
Molecular Weight:227.12

Benzenethiol, 2-(2,2-dibromoethenyl)-4-methyl-

1191415-28-7
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111860-00-5
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$240.00/500mg

Yield:111860-00-5 99%

Reaction Conditions:

with potassium phosphate;copper(l) iodide in tetrahydrofuran at 80;Inert atmosphere;Ullmann condensation;

References:

Newman, Stephen G.;Aureggi, Valentina;Bryan, Christopher S.;Lautens, Mark [Chemical Communications,2009,# 35,p. 5236 - 5238] Location in patent:supporting information; experimental part

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2-BROMO-5-METHYL-1-BENZOTHIOPHENE synthesis

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