2,4-Dichlorophenylacetonitrile synthesis
- Product Name:2,4-Dichlorophenylacetonitrile
- CAS Number:6306-60-1
- Molecular formula:C8H5Cl2N
- Molecular Weight:186.04
773837-37-9
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6306-60-1
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$14.00/5g
Yield:6306-60-1 93%
Reaction Conditions:
in ethanol;water
Steps:
8 Example 8
To a 100 mL round bottom flask was added 2,4-dichlorobenzyl bromide(24 g, 0.1 mol) and ethanol (30 mL) and water (5 mL)Subsequently, sodium cyanide (4.9 g, 0.1 mol) was added and the reaction was stirred. After completion of the reaction, the resulting organic phase was separated and distilled to give 17.30 g of 2,4-dichlorophenylacetonitrile in 93% yield.
References:
Zhejiang Yongtai Pharmaceutical Co., Ltd.;Jin Yizhong;He Renbao;Zhou Guobin;Xie Jianren CN106117028, 2016, A Location in patent:Paragraph 0059; 0060
19719-28-9
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6306-60-1
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$14.00/5g
