2(1H)-Pyrimidinone, 4-(dimethylamino)-1-methyl- synthesis

4synthesis methods

615-77-0 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 75 percent / POCl₃ / 4 h / 70 °C
2: 72 percent / K₂CO₃ / acetonitrile / 1 h / 50 °C

References:

Celewicz;Ciszewski;Golankiewicz [Synthetic Communications,1991,vol. 21,# 14,p. 1489 - 1500]

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