1H-BENZIMIDAZOLE, 5-IODO-2-(TRIFLUOROMETHYL)- synthesis
- Product Name:1H-BENZIMIDAZOLE, 5-IODO-2-(TRIFLUOROMETHYL)-
- CAS Number:3765-86-4
- Molecular formula:C8H4F3IN2
- Molecular Weight:312.03
88-74-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium acetate; acetic acid; Iodine monochloride / 1.75 h / 25 - 90 °C / Inert atmosphere
2: stannous chloride hydrate; hydrogenchloride / water / 3 h / 25 - 65 °C / Inert atmosphere
3: hydrogenchloride / water / 12 h / 80 °C / Inert atmosphere
References:
Alberti, Mariza N.;Polyhach, Yevhen;Tzirakis, Manolis D.;T?dtli, Laura;Jeschke, Gunnar;Diederich, Fran?ois [Chemistry - A European Journal,2016,vol. 22,# 29,p. 10194 - 10202]
20691-72-9
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