Acetamide, N-1,7,8-tris(acetyloxy)octahydro-6-indolizinyl-, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)- synthesis
- Product Name:Acetamide, N-1,7,8-tris(acetyloxy)octahydro-6-indolizinyl-, 1S-(1.alpha.,6.beta.,7.alpha.,8.beta.,8a.beta.)-
- CAS Number:156205-53-7
- Molecular formula:C16H24N2O7
- Molecular Weight:356.38
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 85 percent / pyridine / 0 deg C -> r.t., overnight
2: 30 percent / tributyltin methoxide / tetrahydrofuran / Heating
3: 86 percent / pyridine
4: 56 percent / NaN3 / dimethylsulfoxide / 80 deg C, 1 h; 60 deg C, overnight
5: 81 percent / H2 / 5percent Pd/C / toluene / 24 h
6: 101 percent / pyridine / Ambient temperature
References:
Furneaux, Richard H.;Gainsford, Graeme J.;Mason, Jennifer M.;Tyler, Peter C. [Tetrahedron,1994,vol. 50,# 7,p. 2131 - 2160]
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