1-mercapto-11-hydroxy-3,6,9-trioxaundecane synthesis
- Product Name:1-mercapto-11-hydroxy-3,6,9-trioxaundecane
- CAS Number:90952-27-5
- Molecular formula:C8H18O4S
- Molecular Weight:210.29
![Bis[2-(2-hydroxyethoxy)ethyl] ether](/CAS/GIF/112-60-7.gif)
112-60-7
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90952-27-5
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$200.00/100mg
Yield:-
Steps:
Multi-step reaction with 5 steps
1: 52 percent / pyridine / 12 h / 0 - 20 °C
2: 51 percent / 4-DMAP; Et3N / CH2Cl2 / 20 h / 20 °C
3: 87 percent / dimethylformamide / 2 h / 100 °C
4: 95 percent / HBF4; H2O / acetonitrile / 1 h / 20 °C
5: MeONa / methanol / 2 h / 0 °C
References:
Payre, Nathalie;Cottaz, Sylvain;Boisset, Claire;Borsali, Redouane;Svensson, Birte;Henrissat, Bernard;Driguez, Hugues [Angewandte Chemie - International Edition,1999,vol. 38,# 7,p. 974 - 977]
77544-60-6
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$59.79/1g
90952-27-5
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$200.00/100mg
223611-42-5
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$270.00/100 mg
90952-27-5
61 suppliers
$200.00/100mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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90952-27-5
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$200.00/100mg
223611-40-3
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$198.00/1 g
90952-27-5
61 suppliers
$200.00/100mg