1-Dodecanol, 2-hexyl- synthesis
- Product Name:1-Dodecanol, 2-hexyl-
- CAS Number:110225-00-8
- Molecular formula:C18H38O
- Molecular Weight:270.49
111-87-5
777 suppliers
$6.00/100g
112-30-1
491 suppliers
$5.00/25g
7440-02-0
439 suppliers
$13.19/1slug
110225-00-8
4 suppliers
inquiry
Yield: 90%
Reaction Conditions:
with potassium hydroxide
Steps:
3 EXAMPLE 3
EXAMPLE 3 To 500 grams of decyl alcohol and 500 grams of octyl alcohol, 30.0 grams of potassium hydroxide and 2.0 grams of nickel were added under good agitation. The resulting mixture was heated to 230°-250° C. while water generated from the reaction was removed by distillation. Reaction progress was followed by GLC analysis and the guerbet alcohol product, 2-decyl-octan-1-ol was recovered in greater than 90% yield. The reaction product was then distilled for purification.
References:
GAF Corporation US4830769, 1989, A
111-87-5
777 suppliers
$6.00/100g
112-30-1
491 suppliers
$5.00/25g
2425-77-6
198 suppliers
$28.89/25ml
45235-48-1
28 suppliers
inquiry
110225-00-8
4 suppliers
inquiry
5333-42-6
278 suppliers
$30.00/10g