5-Acetyl-2-bromopyridine synthesis
- Product Name:5-Acetyl-2-bromopyridine
- CAS Number:139042-59-4
- Molecular formula:C7H6BrNO
- Molecular Weight:200.03
624-28-2
732 suppliers
$5.00/5g
127-19-5
865 suppliers
$5.00/25g
139042-59-4
311 suppliers
$6.00/250mg
Yield:139042-59-4 51%
Reaction Conditions:
Stage #1:2,5-dibromopyridine with n-butyllithium in diethyl ether;hexane at -78; for 0.5 h;
Stage #2:N,N-dimethyl acetamide in diethyl ether;hexane at -78 - 20; for 1 h;Further stages.;
References:
El-Deeb, Ibrahim Mustafa;Jae, Chun Ryu;So, Ha Lee [Molecules,2008,vol. 13,# 4,p. 818 - 830]