1-(4-TERT-BUTYLPYRIDIN-2-YL)ETHANONE synthesis
- Product Name:1-(4-TERT-BUTYLPYRIDIN-2-YL)ETHANONE
- CAS Number:41225-63-2
- Molecular formula:C11H15NO
- Molecular Weight:177.24
3978-81-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: dihydrogen peroxide / acetic acid / 90 h / 80 °C
2.1: triethylamine / acetonitrile / 25 h / 100 °C
3.1: diethyl ether; benzene / 1.5 h / 0 °C
3.2: 26 h / 20 °C
References:
Custelcean, Radu;Bonnesen, Peter V.;Duncan, Nathan C.;Zhang, Xiaohua;Watson, Lori A.;Van Berkel, Gary;Parson, Whitney B.;Hay, Benjamin P. [Journal of the American Chemical Society,2012,vol. 134,# 20,p. 8525 - 8534]
23569-17-7
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