1,3,6-HEXANETRICARBONITRILE synthesis
- Product Name:1,3,6-HEXANETRICARBONITRILE
- CAS Number:1772-25-4
- Molecular formula:C9H11N3
- Molecular Weight:161.2
107-13-1
423 suppliers
$17.00/25ML
2941-23-3
158 suppliers
$7.00/1g
1772-25-4
138 suppliers
$45.00/50mg
Yield:1772-25-4 66.9%
Reaction Conditions:
with sodium hydroxide in toluene;
Steps:
6 Example 6
Example 6 Production of 1,3,6-hexanetricarbonitrile by isolating 2-amino-1 -cyclopentene-1 -carbonitrile 583 mg (11 mmol) of acrylonitrile were added at room temperature to a mixture of 1.08 g (10 mmol) of 2-amino-1-cyclopentene-1-carbonitrile (from Example 5), 2 ml (33.7 mmol) of 45% sodium hydroxide solution, 100 mg of Aliquat 336 and 6 ml of toluene and stirred at 50° C. for 22 hours. The mixture was diluted with water, the phases were separated, the organic phase was dried, the solvent was distilled off and the residue was examined by gas chromatography. Trimer yield: 66.9%
References:
US2002/7081,2002,A1
111-69-3
196 suppliers
$14.00/25mL
865-47-4
703 suppliers
$14.00/25g
107-13-1
423 suppliers
$17.00/25ML
1772-25-4
138 suppliers
$45.00/50mg
111-69-3
196 suppliers
$14.00/25mL
107-13-1
423 suppliers
$17.00/25ML
1772-25-4
138 suppliers
$45.00/50mg
141-28-6
371 suppliers
$10.00/100g
1772-25-4
138 suppliers
$45.00/50mg
111-69-3
196 suppliers
$14.00/25mL
1772-25-4
138 suppliers
$45.00/50mg