N-Methyl-d3-N-nitroso-p-toluenesulfonamide is a reagent that easily yields deuterodiazomethane for synthetic purposes1. t is a bench-stable pale yellow powder, soluble in petroleum ether, ether, benzene, alcohol, CHCl3, and CCl4. The generating deuterodiazomethane procedure involves reagent decomposition in a dilute solution catalyzed by an alkali hydroxide.
Synonyms: Diazald-(N-methyl-d3), Diazald-d3
Efficient, Scalable and Economical Preparation of Tris(Deuterium)‐ and 13C‐labelled N‐methyl‐N‐nitroso‐p‐toluenesulfonamide (Diazald?) and Their Conversion to Labelled Diazomethane.
Shields S.; Manthorpe J. J Labelled Comp Radiopharm 2014, 57 (12), 674–679. DOI: 10.1002/jlcr.3231
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