2,4,6-三(二甲氨基甲基)苯酚(90-72-2)核磁圖(¹HNMR)

產(chǎn)品名稱:2,4,6-三(二甲氨基甲基)苯酚

CAS:90-72-2

分子式:C15H27N3O

分子量: 265.39

InChI:InChI=1S/C15H27N3O/c1-16(2)9-12-7-13(10-17(3)4)15(19)14(8-12)11-18(5)6/h7-8,19H,9-11H2,1-6H3

InChIKey: AHDSRXYHVZECER-UHFFFAOYSA-N

Smiles:C1(O)=C(CN(C)C)C=C(CN(C)C)C=C1CN(C)C

Mass

MS-NW-1443          
2,4,6-tris(dimethylaminomethyl)phenol
C15H27N3O           (Mass of molecular ion:    265)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       7.2
      18.0       8.0
      27.0       2.6
      28.0      13.1
      29.0       1.7
      30.0       6.3
      39.0       3.3
      40.0       2.1
      41.0       3.3
      42.0      21.5
      43.0       8.2
      44.0      75.9
      45.0      27.0
      46.0       6.9
      51.0       1.7
      53.0       1.0
      57.0       1.9
      58.0      40.2
      59.0       1.7
      63.0       1.2
      65.0       4.3
      77.0       5.2
      78.0       3.0
      79.0       5.5
      82.0       1.0
      89.0       1.4
      90.0       1.1
      91.0      11.7
      92.0       2.6
      94.0       1.5
     102.0       1.3
     103.0       4.9
     104.0       4.9
     105.0      10.9
     106.0       4.2
     110.0       3.1
     117.0       1.1
     118.0       1.4
     119.0       5.3
     120.0       4.4
     121.0       1.5
     131.0       1.1
     132.0       7.8
     133.0      22.0
     134.0      12.0
     135.0       2.0
     146.0       4.2
     147.0       1.2
     148.0       8.4
     149.0       1.1
     160.0       1.2
     161.0       1.7
     162.0      22.0
     163.0      13.9
     164.0       3.6
     174.0       1.1
     175.0      14.4
     176.0     100.0
     177.0      27.5
     178.0      14.5
     179.0       2.1
     193.0       2.0
     205.0       3.4
     208.0       3.6
     220.0      43.7
     221.0      11.6
     222.0       4.5
     248.0       1.0
     250.0       5.4
     251.0       1.0
     263.0       1.3
     265.0      19.7
     266.0       3.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₂₇ N₃ O	0.05 ml : 0.5 ml CDCl₃
2,4,6-tris(dimethylaminomethyl)phenol

    Assign.     Shift(ppm)

      A             6.948
      B             3.525
      C             3.296
      D             2.283
      E             2.210

     Hz     ppm     Int.

   2777.10   6.949    235
   1412.60   3.535     92
   1408.81   3.526    414
   1317.38   3.297    238
    927.12   2.320     31
    924.68   2.314     46
    923.22   2.311     53
    912.35   2.283   1000
    890.50   2.229     23
    883.42   2.211    696

in CDCl3