13CNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 13CNMR)" />

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143-27-1

十六胺(143-27-1)核磁圖(13CNMR)

產(chǎn)品名稱(chēng):十六胺

CAS:143-27-1

分子式:C16H35N

分子量: 241.46

InChI:InChI=1S/C16H35N/c1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17/h2-17H2,1H3

InChIKey: FJLUATLTXUNBOT-UHFFFAOYSA-N

Smiles:C(N)CCCCCCCCCCCCCCC

  • 圖譜
    Mass 

    MS-NW-0322          
hexadecylamine
C16H35N             (Mass of molecular ion:    241)


       Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          18.0       7.4
      27.0       1.6
      29.0       4.8
      30.0     100.0
      31.0       1.8
      39.0       1.3
      41.0      10.6
      42.0       2.7
      43.0      13.7
      44.0      19.2
      45.0       9.7
      55.0       9.4
      56.0       4.5
      57.0       6.2
      59.0       3.5
      69.0       5.0
      70.0       2.1
      71.0       1.7
      72.0       3.3
      73.0       1.6
      83.0       3.3
      84.0       1.2
      86.0       7.4
      87.0       1.2
      97.0       1.9
     100.0       4.2
     114.0       2.0
     128.0       1.6
     142.0       1.8
     156.0       1.5
     170.0       1.2
     184.0       1.2
     198.0       1.2
     212.0       1.2
     240.0       1.6
     241.0       7.2
     242.0       1.5

90 MHz in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C16 H35 N 0.040 g : 0.5 ml CDCl3
    hexadecylamine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.68
      B             1.76
      C             1.26
      D             0.88
  

         Hz     ppm     Int.


        239.63   2.676     27
    157.44   1.758    115
    112.63   1.258   1000
     78.69   0.879     60

in CDCl3

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CCl4 solution

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KBr disc

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nujol mull

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